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BU/EQ/Boldenone Undecylenate CAS Νο 13103-34-9 για την έγχυση
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Λεπτομέρειες:
Πληρωμής & Αποστολής Όροι:
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Λεπτομερής Περιγραφή Προϊόντος
| CAS αριθ.: | 13103-34-9 | Μοριακός τύπος: | C30H44O3 |
|---|---|---|---|
| Μοριακό βάρος: | 452.67 | EINECS αριθ.: | 236-024-5 |
| Σημείο βρασμού: | 553.2±50.0 °C 760 mmHg | Πυκνότητα: | 1.05±0.1 g/cm3 |
| Λάμψη: | 232,215 ° Γ | Πίεση ατμού: | 0mmHg σε 25°C |
| Προδιαγραφές: | 98% | Εμφάνιση: | ανοικτό κίτρινο ιξώδες υγρό |
| Υψηλό φως: | 13103-34-9,Boldenone Undecylenate |
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BU/EQ/Boldenone undecylenateCAS no: 13103-34-9 yellow liquid for injection
Basic parameter:
Product name :Boldenoneundecylenate
Nickname: Parenabol; Vebonol; Androsta-1, 4-dien-3-one, 17-(1-oxo-10-undecenyl) foxy--(17. Beta.) -; BoldenoneUndeclyenate; 17beta-(1-Oxo-10-undecenyloxy) androsta-1, 4- dien - 3 - one; Estra - 4, 9 - diene - 3 in 2 - dione (boldenoneUndecylenate); BoldenoneUndecylenateInjection; Boldenoeundecylenate
CAS no. : 13103-34-9
Molecular formula: C30H44O3
Molecular weight: 452.67
EINECS no. : 236-024-5
Boiling point: 553.2±50.0 °C at 760 mmHg
Density: 1.05±0.1 g/cm3
Flash: 232.215 ° C
Vapor pressure: 0mmHg at 25°C
Specifications: 98%
Appearance: Light yellow viscous liquid
Certificate of Analysis:
| Product: | Boldenone Undecylenate | |||||||||||
| Batch No.: | 20200503 | Mfg. Date: | 2020-05-19 | Analysis Date: | 2020-05-21 | |||||||
| Quantity: | 50.0KG | CAS No: | 13103-34-9 | Exp. Date: | 2022-05-18 | |||||||
| Storage: | Preserve in tight, light-resistant containers. | Standard: | IN-HOUSE | |||||||||
| ITEM AND RESULT | ||||||||||||
| Item | Specification | Result | ||||||||||
| Characters |
From pale yellow to clear at room termp. Odourless or with slight characteristic odour |
Complies | ||||||||||
| Solubility | Practically insoluble in water, soluble in ethanol, chloroform, acetone dioxan, vegetable oils | Complies | ||||||||||
| Identification | A. UV | Complies | ||||||||||
| B. IR | ||||||||||||
| C. TLC | ||||||||||||
| Specific Rotation | +28.0° ~ +35.0° | +30.9° | ||||||||||
| Density | 1.020~1.035 | 1.028 | ||||||||||
| Loss on Drying | ≤0.5% | 0.31% | ||||||||||
| Free Undecylenate | ≤0.45% | 0.29% | ||||||||||
| Related Substances | Total Impurities ≤3.0% | 0.87％ | ||||||||||
| Assay | ≥97% (HPLC) | 99.13% | ||||||||||
| Conclusion: | Complies with the IN-HOUSE Standard | |||||||||||
| Operator | Review | Q.C. Manager | ||||||||||
Product series:
Application:
Baodanone undecenoate is a chemical intermediate. The intermediate L, 4-androstene-17SS-3-11enoate, could be prepared from testosterone undecenoate as starting material, and further reacted with glacial acetic acid, pentanol and mercury to produce baotanone undecenoate.
Step 1: The synthesis of L, 4- androstene-17SS-3-eleven enolates
In 200 ml of tert-butyl ether, 4.54 g of 44-androenone 17 -3-11enone [testosterone undecenone] was added. 6.0g mercury was added in a nitrogen atmosphere and stirred continuously. 3.70g of selenium dioxide was dissolved in the mixture. The cooled reaction solution was filtered to separate selenium, mercury selenide and mercury, diluted with ethyl acetate, and then shaken repeatedly with ammonium sulfide and sodium carbonate solutions, washed with water, dried and evaporated by sodium sulfate. The result is 4.1g of coarse L, 4-androstenediene-17/3-3-11-enonate, which is a thick brown oil. It was dissolved in hexane and adsorbed under the action of alumina. Eluent with hexane, hexane-benzene 1:1 and benzene was used to obtain 3.2GL, 4-androstene-17SS-3-11enoate.
Step 2: Synthesis of baodanone undecenoate
4.5g l, 4-androstene-17SS-3-11-enenate, amyl alcohol and 5.0ml glacial acetic acid were added to 200mL solution. 12.0g mercury was added to stir vigorously under nitrogen atmosphere. 7.4g selenium dioxide was dissolved in 330ml mixture at reflux-temperature and pentanol was added. The mixture is then stirred in a nitrogen atmosphere to reflux for another 20 hours. Cooling reaction solution, mercury selenide and mercury separation, diluted with ethyl acetate, thoroughly washed with ammonium sulfide and soda solution, dried and evaporated. The obtained crude product was dissolved in hexane and coated with alumina in hexane. It was eluted with hexane, hexane - benzene 1∶1 and benzene to obtain 2.7g baotanone undecenoate.
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